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Table 7.1 SCSI versus Fibre Channel TECHNOLOGY Ultra640 SCSI Fibre Channel DATA TRANSFER RATE 640MB/sec 2GB/sec NUMBER OF DEVICES 16 No limit MAXIMUM DISTANCE 82 feet end-to-end 80 kilometers between devices and beyond with new technologies

3.1. INTRODUCTION The quantitation of enzymes and substrates has long been of critical importance in clinical chemistry, since metabolic levels of a variety of species are known to be associated with certain disease states. Enzymatic methods may be used in complex matrices, such as serum or urine, due to the high selectivity of enzymes for their natural substrates. Because of this selectivity, enzymatic assays are also used in chemical and biochemical research. This chapter considers quantitative experimental methods, the biochemical species that is being measured, how the measurement is made, and how experimental data relate to concentration. This chapter assumes familiarity with the principles of spectroscopic (absorbance, uorescence, chemiand bioluminescence, nephelometry, and turbidimetry), electrochemical (potentiometry and amperometry), calorimetry, and radiochemical methods. For an excellent coverage of these topics, the student is referred to Daniel C. Harris, Quantitative Chemical Analysis (6th ed.). In addition, statistical terms and methods, such as detection limit, signal-to-noise ratio (S/N), sensitivity, relative standard deviation (RSD), and linear regression are assumed familiar; 16 in this volume discusses statistical parameters. Biochemical literature often uses the terms detection limit and sensitivity interchangeably. We will use detection limit to describe the minimum detectable amount of analyte, which is that amount required to generate a signal that is two or three standard deviations in magnitude above the signal obtained for a reagent blank solution (i.e., a blank that contains everything except the analyte). The slope of the calibration curve of signal versus analyte concentration is de ned as the sensitivity of a quantitative assay; this slope describes how sensitive the assay is to changes in analyte concentration. It follows from this de nition that, for nonlinear calibration curves, sensitivity is a function of concentration. These de nitions conform to conventions in analytical chemistry.

Multipathing is the connection of a single host to a single disk array with more than one data path. This technology requires multiple interface cards in the host, and a disk array that has sufficient inputs to support all the connections. Data transfer rates can be increased nearly linearly (that is, two 80MB/second connections yield an effective transfer rate of almost 160MB/second) if both connections are active all the time. If one of the connections fails, the other should be able to take over the full data transfer load without interruption, limited only by its own remaining throughput. Connections may fail due to a cable breaking or being removed, or because an interface card or controller in either the disk array or in the host has failed. All of these failures will be transparent in a properly configured multipathed environment. Commercial examples of multipathing include VERITAS s DMP feature in their Volume Manager product, and EMC s PowerPath. A simple example of multipathing can be found in Figure 7.4.

Bianalytical Chemistry, by Susan R. Mikkelsen and Eduardo Corton ISBN 0-471-54447-7 Copyright # 2004 John Wiley & Sons, Inc.

Multihosting is the connection of one set of disks to two or more servers at the same time. Both servers can see and access the disks, but generally will not at the same time. Multihosting is most commonly used in a clustered environment, enabling the takeover server to get data that is as up-to-date as possible. For more on clustering, please see 17, Local Clustering and Failover. In a SCSI environment, multihosting, accomplished through multi-initiated SCSI, is an exception that is generally found only in clustered environments. It is the norm in the FC world.

A disk array is a single enclosure or cabinet, containing slots for many disks. The array may use SCSI or Fibre Channel internally to address its disks, and may use SCSI or Fibre Channel to connect to its host(s). The same array may have SCSI disks internally, while connecting to its host(s) via Fibre Channel.